Technology
The MESA-7220V2 measures both sulfur and chlorine in petroleum based products using the Monochromatic EDXRF method. A monochromatic X-ray source is used in order to obtain an ultra-low noise background which affords the best detection limits for both sulfur and chlorine.The detector window size was increased to collect more fluorescent X-rays and thus achieve lower level ppm values. This provides excellent, repeatable performance at both low and high concentrations of both elements. By adjusting the angle of the graphite crystal, the excitation beam can be measured to excite sulfur in the sample,increasing sensitivity.
Key Features :
-
Dynamic Analysis Range:
• Sulfur: 0.7 ppm - 10.0Wt%
• Chlorine: 0.6 ppm - 10.0Wt% - Auto Ranging for extended curves.
- No purge gases required.
- Maximum 60 calibration curves and 300 data points per curve.
- Calibration curves can be edited after they have been saved.
- Measurement times from 30 – 999 sec.
- Measurement repeats from 1 – 99 times.
- Oxygen correction feature eliminates interference which can affect Sulfur readings.
- Various sample types* [Solids, Liquids, Powders, Pastes, Pellets, and Films] can be measured.
- Can program up to 20 Admin & User accounts.
- User replaceable Kapton window.
- Micrometer adjustment of graphite crystal angle for better sensitivity.
- Stand-alone PC to allow software updates electronically.
- Built-in interlocks to protect end-user from X-rays.
- Silicon Drift Detector/X-ray Beryllium Window.
Measuring Principle :
The pulse-height analyzer counts the number of electric pulses from the X-rays which come into each window, during a given time, and obtains the integrated values. These values are then converted into a count per second and used in the calculations. The quantities of X-rays which come into the windows are called the quantity of fluorescent X-rays from sulfur, NS (cps), the quantity of fluorescent X-rays from chlorine, NCI (cps), and the quantity of scattered X-rays, NB (cps), respectively
The analyzer calculates the K value, which is the ratio of NS to NB (K = NS/NB) or NCI to NB (K = NCI/NB) and uses it as the measured value. The determined value (ppm) is read from the K value compared to the calibration curve.
When the high-voltage power is sent to the X-ray tube,the primary X-rays are radiated from the X-ray tube to the curved crystal. X-rays irradiated to the curved crystal are monochromatied by the curved crystal and irradiated on the sample cell. Some of the radiated X-rays excite the sulfur and chlorine atoms, generating fluorescent X-rays. These fluorescent and any remaining scattered X-rays are detected by the X-ray detector. In the X-ray detector, electric pulses are generated in proportion to the energy of the incoming X-rays. These electric pulses are strengthened by the pulse amplifier before being sent as a voltage signal to the pulse-height analyzer.
Specifications :
Instrument Dimensions | Inch | mm |
---|---|---|
Width | 11.69 | 297 |
Depth | 16.54 | 420 |
Height (Closed) | 16.54 | 420 |
Height (Open) | 29.49 | 749 |
Instrument Mass |
---|
32 kg / 70.55 lb (PC, display monitor, and printer are not included) |
Principle | X-ray Fluorescence analysis (Monochromatic EDXRF) |
Sample | Petroleum products |
Elements to Measure | Sulfur (S) and Chlorine (Cl) |
Height (Open) | 29.49 |
Measurement Range | 0.00 – 100,000 ppm |
Detection Limit | S: 0.7 ppm Cl: 0.6 ppm |
Sample Volume | 7 – 10 ml for each sample cell |
Sample Chamber | Atmospheric Conditions |
X-ray Tube | Ag Target |
Detector | Silicone Drift Detector (SDD) Energy resolution at Mn-Kα ≤ 175 eV |
Vacuum Level | ≤ 4 kPa, Diaphragm Pump |
Conformity Standards | ASTM D7220 / D4294 ISO 8754 / 13032 / 20847 |
Printer | |
---|---|
Model | CT-S4000 made by CITIZEN |
Paper / Paper width | Line thermal printer (External) / 112mm / 4.4 inch |
PC | |
---|---|
CPU | Intel Core i5-8500 or faster |
OS | Microsoft Windows 10 Pro, 64 bit,English (US) |
Memory | 4GB or more |
Storage | 1TB or more |
Display Unit | |
---|---|
Resolution | Full HD (1920 x 1080) |
Panel Size | 17 - 23 inch |
Request Quote